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Optimised recovery of double-base smokeless powder residues analysed by TV-SPME/GC-MS

Curtin University
Dana Bors (Aggregated by) Georgina Sauzier (Associated with, Aggregated by) John Goodpaster (Aggregated by) Jordan Ash (Aggregated by) Simon Lewis (Aggregated by)
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ctx_ver=Z39.88-2004&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Adc&rfr_id=info%3Asid%2FANDS&rft_id=info:doi10.25917/5b69534b232c1&rft.title=Optimised recovery of double-base smokeless powder residues analysed by TV-SPME/GC-MS&rft.identifier=10.25917/5b69534b232c1&rft.publisher=Curtin University&rft.description=This dataset was collected by Georgina Sauzier at Indiana University-Purdue University, Indianapolis in 2015 as part of a PhD exchange placement, as described in the linked article. Simulated smokeless gunpowder residues were analysed using total vaporisation (TV)-SPME/GC-MS as part of a central composite design. Optimised parameters for recovery of the target components were then tested using real residues generated from a pipe bomb detonation. Peak areas were integrated using Thermo Xcalibur v2.0.7. The central composite design was created and analysed using Design Expert v10.&rft.creator=Dana Bors&rft.creator=Georgina Sauzier&rft.creator=John Goodpaster&rft.creator=Jordan Ash&rft.creator=Simon Lewis&rft.date=2018&rft.relation=http://doi.org/10.1016/j.talanta.2016.04.048&rft_rights=Free for re-use under a CC BY: Attribution 4.0 licence http://creativecommons.org/licenses/by/4.0/&rft_rights=CC BY: Attribution 4.0 http://creativecommons.org/licenses/by/4.0/&rft_subject=forensic science&rft_subject=explosives&rft_subject=gas chromatography-mass spectrometry&rft_subject=experimental design&rft_subject=optimisation&rft_subject=Forensic Chemistry&rft_subject=CHEMICAL SCIENCES&rft_subject=OTHER CHEMICAL SCIENCES&rft_subject=Separation Science&rft_subject=ANALYTICAL CHEMISTRY&rft.type=dataset&rft.language=English Access the data
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This dataset was collected by Georgina Sauzier at Indiana University-Purdue University, Indianapolis in 2015 as part of a PhD exchange placement, as described in the linked article. Simulated smokeless gunpowder residues were analysed using total vaporisation (TV)-SPME/GC-MS as part of a central composite design. Optimised parameters for recovery of the target components were then tested using real residues generated from a pipe bomb detonation.

Peak areas were integrated using Thermo Xcalibur v2.0.7. The central composite design was created and analysed using Design Expert v10.

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Analytical Chemistry | Chemical Sciences | Forensic Chemistry | Other Chemical Sciences | Separation Science | experimental design | explosives | forensic science | gas chromatography-mass spectrometry | optimisation |

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